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Synthesis of Cyclopropanecarbonyl chloride
Author(s): 
Pages: 36-38
Year: Issue:  7
Journal: CHEMICAL INDUSTRY TIMES

Keyword:  环丙烷甲酸异丙酯环丙烷甲酸环丙烷甲酰氨合成;
Abstract: 环丙烷甲酸异丙酯因异丙基的位阻很大,所以其很难水解,即使加热回流12 h,得率也只有68.6%,选用合适的相转移催化剂使得率超过了84%.由环丙烷甲酸制备环丙烷甲酰氯比较简单,文献报道得率为94.08%,通过对其合成条件的优化,使得率超过了97.2%.
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