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An organic-inorganic hybrid compound based on arsenatomolybdates and Ni complexes
Author(s): 
Pages: 57-61
Year: Issue:  1
Journal: Chemical Research

Keyword:  polyoxometalatehydrothermalcrystal structurearsenamolybdate;
Abstract: A novel arsenamolybdate [Ni(dien)2 ]2 [As6 NiMo6 O30 ] ? 2H2 O (1) (dien = diethyl‐enetriamine) ,has been prepared by hydrothermal methods and structurally characterized by el‐emental analysis ,IR ,TG analysis and single‐crystal X‐ray diffraction analysis .Compound 1 crystallizes in the monoclinic space group P2 (1)/n .The structure of 1 is constructed from [As6 NiMo6 O30 ]4 - anionic clusters and [Ni(dien)2 ]2 + complex subunits .
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