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Process of Chemical Synthesis and Explore about Nickel Phthalocyanine Crystals
Author(s): XIA Dao-cheng, REN Xu-wen, LI Wan-cheng, Institute of Organic Chemistry, Shanxi Datong University, State Key Laboratory of Integrated Optoelectronics, College of Electronic Science and Engineering, Jilin University
Pages: 1140-
1142+1145
Year: 2015
Issue:
12
Journal: Chemical Reagents
Keyword: nickel phthalocyanine; synthesis; reaction conditions;
Abstract: The solvothermal synthesis method of Ni Pc single crystals was studied by using 1,3-dimino-isoindoline and Ni( Ac O)2·2H2O as starting materials in this article. The influences of the different temperatures,reaction time,solvent volumes and catalyst on the crystal yield were also discussed. Then the best reaction conditions which were temperature,time and catalyst were found.Thus,the synthetic method of nickel phthalocyanine crystals in industry was provided,and the highest Ni Pc crystal yield was under270 ℃ for 8 h in 14 m L quinoline.
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