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Issue:
Study on the Synthesis of Acyl Azides
Author(s):
Wen Tianzhen
,
Liu Yi
,
Zeng Hongyao
,
College of Chemistry
,
Leshan Normal University
Pages:
88
-
90
Year:
2015
Issue:
8
Journal:
Guangdong Chemical Industry
Keyword:
benzoyl chloride
;
acyl azide
;
sodium azide
;
polyethylene glycol
;
organic synthesis
;
Abstract:
Acyl azides synthetized from aromatic acyl chloride with sodium azide in various solvent at room temperature was exploreed. It was found that acetone, acetonitrile, PEG-200 and PEG-400 is four kinds good solvent for the reaction. The method has the advantages such as short reaction time, high reaction yield, easy to operate and convenient work-up.
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