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kang de ling jiao nang bao ceng se pu fa de zhi liang kong zhi
Author(s): 
Pages: 56-57
Year: Issue:  S1
Journal: Chinese Journal of Public Health Engineering

Keyword:  康得灵胶囊薄层色谱法质量控制;
Abstract: 康得灵胶囊是我院自制的中药制剂,主要成分为黄芪、黄连、黄柏,具有清热燥湿、肠道消炎的功能。为了确保制剂质量,采用薄层色谱法鉴别其中的盐酸小檗碱、黄芪等主要成分,为制剂生产的质量控制提供有效依据。1仪器与试药1·1仪器QY-20型三用紫外分析仪(上海澳瑞德仪器厂),硅胶G薄层板。1·2试药甲醇、醋酸丁酯、甲酸、正丁醇、氯仿、硫酸乙醇。对照品:盐酸小檗碱盐、黄芪甲苷对照品、黄芪对照药材(中国药品生物制品检验所)。2结果与讨论2·1黄连、黄柏的薄层鉴别2·1·1供试品制备取本品15粒倾出内容物,加甲醇20 m l密塞振摇30 m in滤过,滤液为供试品。2·1·2阴性对照品溶液的制备取不含黄连、黄柏
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