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A New Method to Synthesize 3,3'-Diamino-4,4'-azoxyfurazan (DAOAF)
Author(s): 
Pages: 273-275
Year: Issue:  2
Journal: Chinese Journal of Energetic Materials

Keyword:  有机化学33'-二氨基-44'-氧化偶氮呋咱3-氨基-4-甲酰胺基呋咱34-二甲酰胺基呋咱合成;
Abstract: 以3,4-二氨基呋咱为原料,经过中间体3-氨基-4-甲酰胺基呋咱或3,4-二甲酰胺基呋咱,以1,4-二氧六环为溶剂,30%双氧水为氧化剂,加热回流4h,得到产物3,3’-二氨基-4,4’-氧化偶氮呋咱(DAOAF),产率分别为97%或89%.并通过1H NMR、13C NMR、IR和El对产物进行了表征.
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