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Synthesis and crystal structure of [Cu(dmbzpymt)]6·2CHCl3 (dmbzpymtH = 5-benzyl-4,6-dimethylpyrimidine-2-thione)
Author(s): 
Pages: 91-94
Year: Issue:  3
Journal: Journal of Suzhou University Natural Science

Keyword:  46-二甲基-5-苄基-2-嘧啶硫醇铜化合物晶体结构合成;
Abstract: 4,6-二甲基-5-苄基-2-嘧啶硫醇(dmbzpymtH)与CuI和NaOH反应得到化合物[Cu(dmbzpymt)]6·2CHCl3 (1·2CHCl3),该化合物通过元素分析、红外光谱等表征.X射线衍射法测得该晶体属于三斜晶系,空间群为Pī,晶胞参数:a = 1.5314(3) nm,b= 1.5429(3) nm,c = 1.9706(4) nm,α = 108.401(4)°,β =91...
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