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Thermal Behavior and Nonisothermal Decomposition Reaction Kinetics of 4-Amino-1,2,4-triazole Copper Complex
Pages: 368-371
Year: Issue:  4
Journal: Chinese Journal of Energetic Materials

Keyword:  physical chemistrycopper complex4-amino-124-triazolethermal decomposition mechanismnonisothermal reaction kinetics;
Abstract: 利用4-氨基-1,2,4-三唑(4-ATz)与二水氯化铜合成了标题化合物(C2N4H4)2CuCl2·H2O,采用元素分析和红外光谱分析对配合物进行了结构表征,用DSC和TG-DTG研究了配合物的热行为及主放热分解阶段的动力学.结果表明,金属离子与配体的化学计量比为12.配合物的主要分解阶段由机理函数f(α)=32(1-α)[-ln(1-α)]1/3控制,反应速率方程为: dα/dt=1021....
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