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RP HPLC METHOD FOR DETERMINATION OF SERUM MOCLOBEMIDE CONCENTRATION
Author(s): 
Pages: 261-262
Year: Issue:  3
Journal: Acta Academiae Medicinae Shandong

Keyword:  吗氯贝胺 血液 色谱法 高压液相;
Abstract: 以乙腈水(30∶70, V/ V)为流动相,氯霉素为内标,采用反相高效液相色谱法测定吗氯贝胺浓度。血吗氯贝胺在碱性条件下用乙醚提取,甲醇溶解残留物,在 004~4.0μg/m l浓度范围内线性关系良好,r= 0.9996,相对平均回收率为 970% ,日内 R S D(% )26~3.5,日间 R S D(% )3.7~4.2,最低检出浓度004μg/m l。本法快速、准确,灵敏度高,专一性强,适用于吗氯贝胺临床监测及科研需要。
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