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Determination of related substances in azithromycin injection by RP-HPLC
Author(s):
SUN Bei-bei
,
XU Jing
,
XU Kang-kang
Pages:
1491
-
1492
Year:
2009
Issue:
12
Journal:
Anhui Medical and Pharmaceutical Journal
Abstract:
目的 建立注射用阿奇霉素有关物质的新检测方法.方法 采用反相高效液相色谱法检测注射用阿奇霉素中有关物质.液相色谱条件为:以Shim-pack CLC-ODS不锈钢柱(250 mm×4.6 mm,5 μm)为色谱柱,以0.05 mol·L-1K2HPO4-乙腈(40:60)为流动相,流速1.0 ml·min-1,柱温40℃,检测波长215 nm.结果 阿奇霉素有关物质的检测限度为2.5%,阿奇霉素主...
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