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Synthesis and micro-structrual characterization of Bi_(3.15) Nd_(0. 85) Ti_3O_(12) nanotube arrays
Author(s): ZOU Yazuo, HU Yongming, HU Zhenglong, ZHOU Di, QIAN Zheli, WANG Zuo, GU Haoshuang
Pages: 375-
378
Year: 2009
Issue:
4
Journal: Journal of Hubei University(Natural Science Edition)
Keyword: Bi_(3.15)Nd_(0.85)Ti_3O_(12); nanotube array; sol-gel; AAO template;
Abstract: 采用溶胶-凝胶法,在孔径为100 nm的阳极氧化铝模板中制备了Bi_(3.15)Nd_(0.85)Ti_3O_(12)(BNdT)纳米管阵列.通过XRD、SEM、TEM、HRTEM、SAED和Raman光谱测试手段对纳米管阵列的物相、微结构和声子振动特性进行了表征.研究表明,所合成BNdT纳米管为钙钛矿相多晶结构,纳米管外径约为100 nm,管壁厚约10 nm,长度达几个微米.Raman光谱分析表...
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