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Synthetic Improvement of DNPP
Author(s): 
Pages: 205-208
Year: Issue:  3
Journal: CHINESE JOURNAL OF ENERGETIC MATERIALS

Keyword:  有机化学富氮化合物二硝基吡唑并吡唑(DNPP)合成;
Abstract: 以乙酰丙酮与水合肼为原料,经脱水缩合、一次硝化、还原、重氮化、环化、二次硝化、氧化、脱羧硝化等反应合成了DNPP,收率9.3%,并采用元素分析、红外光谱、核磁共振进行了表征;初步探讨了合成条件及环化反应历程.
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